Evidence mapPaperPMID 30940446Full record

ArticleAnalytical biochemistry2019

Fast LC-MS quantitation of glucose and glycerol via enzymatic derivatization.

Eric Chiles, Yujue Wang, Katarzyna M Kalemba, Hyokjoon Kwon, Fredric E Wondisford, Xiaoyang Su

Open access · greenAbstract read
In one paragraph

Article in Analytical biochemistry, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.

0numbers the graph read from it
0cells of the map it votes in
7citing papers in PubMed
0.8field-weighted citation impact, top 29% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

7 citing papers in PubMed, 25 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 1 institution in 1 country.

Eric ChilesRutgers Cancer Institute of New Jersey, New Brunswick, NJ, 08903, USA.
Yujue WangDepartment of Medicine, Rutgers-Robert Wood Johnson Medical School, New Brunswick, NJ, 08901, USA.
Katarzyna M KalembaDepartment of Medicine, Rutgers-Robert Wood Johnson Medical School, New Brunswick, NJ, 08901, USA.
Hyokjoon KwonDepartment of Medicine, Rutgers-Robert Wood Johnson Medical School, New Brunswick, NJ, 08901, USA.
Fredric E WondisfordDepartment of Medicine, Rutgers-Robert Wood Johnson Medical School, New Brunswick, NJ, 08901, USA.
Xiaoyang SuRutgers Cancer Institute of New Jersey, New Brunswick, NJ, 08903, USA; Department of Medicine, Rutgers-Robert Wood Johnson Medical School, New Brunswick, NJ, 08901, USA. Electronic address: xs137@rwjms.rutgers.edu.
Rutgers, The State University of New Jersey · US

Funding

The effects of obesity and GLP-1R/GIPR agonists on early-onset breast cancer riskP30CA072720 · NCI · UNIV OF MED/DENT NJ-R W JOHNSON MED SCH · 1997 to 2025
$27.3M
Control of Beta Cell Function by Co-activatorsR01DK063349 · UNIVERSITY OF CHICAGO · 2002 to 2005
$1.9M
NCI NIH HHS P30 CA072720NIDDK NIH HHS R01 DK063349
6 · The paper itself

Abstract

Glucose and glycerol are important circulating metabolites. Due to poor ionization and/or ion suppression, the liquid chromatography-mass spectrometry (LC-MS) detection of glucose and glycerol presents challenges. Here, we propose an efficient LC-MS method of quantitative glucose and glycerol detection via enzymatic derivatization to glucose-6-phosphate and sn-glycerol-3-phosphate, respectively. This derivatization protocol can be used to measure the concentrations of glucose production in a plethora of sample types for metabolic analysis and is compatible with the general metabolomics workflow. This novel approach allows us to quantitatively study glucose and glycerol metabolism using stable isotope tracers in vivo.

Indexed as

Chromatography, LiquidEnzymesGlucoseGlycerolLimit of DetectionMass SpectrometryReproducibility of ResultsEnzymesGlucoseGlycerol

Identifiers

PMID30940446
PMCPMC6504547
OpenAlexW2934125469

What Socratic holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.