Evidence mapPaperPMID 37067885Full record

ArticleJournal of chemical education2023

Introduction to Pharmaceutical Co-amorphous Systems Using a Green Co-milling Technique.

Joana F C Silva, Mário T S Rosado, Teresa M R Maria, Pedro S Pereira Silva, Manuela Ramos Silva, M Ermelinda S Eusébio

Open access · hybridAbstract read
In one paragraph

Article in Journal of chemical education, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.

0numbers the graph read from it
0cells of the map it votes in
5citing papers in PubMed
2.1field-weighted citation impact, top 13% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

5 citing papers in PubMed, 19 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 1 institution in 1 country.

Joana F C SilvaCQC-IMS, Dep. de Química, Universidade de Coimbra, Rua Larga, Coimbra 3004-535, Portugal.
Mário T S RosadoCQC-IMS, Dep. de Química, Universidade de Coimbra, Rua Larga, Coimbra 3004-535, Portugal.ORCID https://orcid.org/0000-0001-5782-8819
Teresa M R MariaCQC-IMS, Dep. de Química, Universidade de Coimbra, Rua Larga, Coimbra 3004-535, Portugal.
Pedro S Pereira SilvaCFisUC, Dep. de Física, Universidade de Coimbra, Rua Larga, Coimbra 3000-370, Portugal.
Manuela Ramos SilvaCFisUC, Dep. de Física, Universidade de Coimbra, Rua Larga, Coimbra 3000-370, Portugal.ORCID https://orcid.org/0000-0001-9555-8856
M Ermelinda S EusébioCQC-IMS, Dep. de Química, Universidade de Coimbra, Rua Larga, Coimbra 3004-535, Portugal.ORCID https://orcid.org/0000-0002-5515-7721
University of Coimbra · PT

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The concept of co-amorphous systems is introduced in an integrated laboratory experiment, designed for advanced chemistry students, using solvent-free, environmentally friendly mechanochemistry. The dual-drug naproxen-cimetidine co-amorphous system (NPX-CIM) is investigated as an example of the emergent field of medicinal mechanochemistry. Students are trained in solid-state characterization techniques including X-ray powder diffraction, Fourier-transform infrared spectroscopy, and thermal analysis by differential scanning calorimetry. This lab experiment also provides an opportunity to discuss the relevance of different solid forms of pharmaceutics, emphasizing particular properties of disordered materials. This experiment can easily fit the curriculum of any Chemistry or Pharmacy master level degree in courses dealing with instrumental analysis, solid state chemistry, or green chemistry, for classes of 6 to 18 students, in a 5-h lab session. Suggestions to adapt it to the use of a single characterization technique are provided.

Identifiers

PMID37067885
PMCPMC10100544
OpenAlexW4360608371

What Socratic holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.