Evidence map›Paper›PMID 37495926›Full record

ArticleAnalytical sciences : the international journal of the Japan Society for Analytical Chemistry2023

Voltammetric determination of doxycycline in feedstock using modified carbon screen-printed electrode.

M S Tiwari, R G Thorat, B B Popatkar, V V Borge, A K Kadu

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Article in Analytical sciences : the international journal of the Japan Society for Analytical Chemistry, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

M S TiwariUniversity Department of Chemistry, University of Mumbai, Santacruz (East), Mumbai, Maharashtra, 400 098, India.
R G ThoratUniversity Department of Chemistry, University of Mumbai, Santacruz (East), Mumbai, Maharashtra, 400 098, India.
B B PopatkarUniversity Department of Chemistry, University of Mumbai, Santacruz (East), Mumbai, Maharashtra, 400 098, India.
V V BorgeUniversity Department of Chemistry, University of Mumbai, Santacruz (East), Mumbai, Maharashtra, 400 098, India.
A K KaduUniversity Department of Chemistry, University of Mumbai, Santacruz (East), Mumbai, Maharashtra, 400 098, India. kadu.arun@chemistry.mu.ac.in.ORCID http://orcid.org/0000-0001-9499-1551

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

In this work, we describe the development of an electrochemical sensing platform that employs electrochemically reduced graphene oxide (ErGO) and gold (Au) deposited on a screen-printed carbon electrode (SPCE) to synthesize Au/ErGO/SPCE for the determination of the antibiotic drug doxycycline (DC). A modified Hummer's approach was adopted to initially prepare graphene oxide, which was then characterized by using powder XRD, FTIR, and UV spectroscopy before being utilized for modification on SPCE. Cyclic voltammetry was performed to form ErGO on SPCE to give ErGO/SPCE followed by electrodeposition of gold to get a final modified electrode Au/ErGO/SPCE. The effect of experimental conditions, like scan rate and pH on the electrochemical behavior of DC for Au/ErGO/SPCE, was evaluated. Square wave voltammetry (SWV) and cyclic voltammetry (CV) measurements were used to assess the electro-oxidation of DC on Au/ErGO/SPCE, and the electrochemical reaction conditions were also optimized. Furthermore, Au/ErGO/SPCE-based electrochemical sensors showed good recovery and high accuracy for DC determination in the complex food matrix and blood serum. The limit of detection (LOD), the limit of quantification (LOQ), and the linear calibration range of DC on Au/ErGO/SPCE under optimum experimental conditions were 0.124 µm, 0.415 µm, and 1-100 µm respectively, with high sensitivity of 0.194 μA μM

Indexed as

Anti-Bacterial AgentsCarbonDoxycyclineElectrochemical TechniquesElectrodesGoldGraphiteLimit of DetectionOxidation-ReductionAnti-Bacterial AgentsCarbonDoxycyclineGoldgraphene oxideGraphiteChickenDoxycycline hyclateElectrochemical sensorElectro-deposited goldSquare wave voltammetry

Identifiers

PMID37495926

What Socratic holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.