Evidence map›Paper›PMID 38930787›Full record

ArticleMolecules (Basel, Switzerland)2024

Structural Characterization and Electrochemical Studies of Selected Alkaloid N-Oxides.

Olha Dushna, Liliya Dubenska, Andrzej Gawor, Jakub Karasińki, Oksana Barabash, Yurii Ostapiuk, Mykola Blazheyevskiy, Ewa Bulska

Abstract read
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In one paragraph

Article in Molecules (Basel, Switzerland), 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Olha DushnaBiological and Chemical Research Centre, Faculty of Chemistry, University of Warsaw, Żwirki i Wigury 101, 02-093 Warsaw, Poland.ORCID 0000-0002-0552-4247
Liliya DubenskaFaculty of Chemistry, Ivan Franko National University of Lviv, Kyryla i Mefodiya 6, 79-005 Lviv, Ukraine.ORCID 0000-0002-8321-6020
Andrzej GaworBiological and Chemical Research Centre, Faculty of Chemistry, University of Warsaw, Żwirki i Wigury 101, 02-093 Warsaw, Poland.ORCID 0000-0001-9578-4968
Jakub KarasińkiBiological and Chemical Research Centre, Faculty of Chemistry, University of Warsaw, Żwirki i Wigury 101, 02-093 Warsaw, Poland.
Oksana BarabashFaculty of Chemistry, Ivan Franko National University of Lviv, Kyryla i Mefodiya 6, 79-005 Lviv, Ukraine.
Yurii OstapiukFaculty of Chemistry, Ivan Franko National University of Lviv, Kyryla i Mefodiya 6, 79-005 Lviv, Ukraine.
Mykola BlazheyevskiyDepartment of General Chemistry, National University of Pharmacy, Valentynivska 4, 61-168 Kharkiv, Ukraine.ORCID 0000-0002-8032-347X
Ewa BulskaBiological and Chemical Research Centre, Faculty of Chemistry, University of Warsaw, Żwirki i Wigury 101, 02-093 Warsaw, Poland.ORCID 0000-0003-4872-5521

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

In this work, we synthesized and confirmed the structure of several alkaloid N-oxides using mass spectrometry and Fourier-transform infrared spectroscopy. We also investigated their reduction mechanisms using voltammetry. For the first time, we obtained alkaloid N-oxides using an oxidation reaction with potassium peroxymonosulfate as an oxidant. The structure was established based on the obtained fragmentation mass spectra recorded by LC-Q-ToF-MS. In the FT-IR spectra of the alkaloid N-oxides, characteristic signals of N-O group vibrations were recorded (bands in the range of 928 cm⁻

Indexed as

AlkaloidsElectrochemical TechniquesOxidation-ReductionOxidesElectrodesMass SpectrometryMolecular StructureSpectroscopy, Fourier Transform InfraredAlkaloidsOxidesalkaloidsFT-IR spectroscopymass spectrometryN-oxide alkaloidssynthesis

Identifiers

PMID38930787
PMCPMC11205554

What Socratic holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.