ArticleJournal of synchrotron radiation2025
A low-background setup for in situ X-ray total scattering combined with fast scanning calorimetry.
Article in Journal of synchrotron radiation, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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9 authors.
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Abstract
We demonstrate a setup, combining fast scanning calorimetry with X-ray total scattering at a synchrotron beamline, allowing for in situ characterizations of the nano-scale structure of samples during and after temperature scans. The setup features a portable vacuum chamber providing a high signal-to-background ratio even on amorphous samples, which enables the observation of detailed structural changes between different sample states. We present three use cases, including one that leverages the high cooling rate of 10
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