Evidence map›Paper›PMID 40893464›Full record

ArticleJournal of materials science2025

High-resolution DIC analysis of in situ strain and crack propagation in coated AZ31 magnesium alloys under mechanical loading.

Berzah Yavuzyegit, Katerina Karali, Sarah Davis, Benjamin Morrison, Suleyman Karabal, Kemal Balandiz, Nigel Smith, Sergey Usov, Pavel Shashkov, Roxane Bonithon and 1 more

Abstract read
In one paragraph

Article in Journal of materials science, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors.

Berzah YavuzyegitFaculty of Science and Health, School of Medicine, Pharmacy and Biomedical Sciences, University of Portsmouth, St Michael's Building, White Swan Road, Portsmouth, PO1 2DT UK.ORCID 0000-0003-0759-780X
Katerina KaraliSchool of Mechanical & Design Engineering Faculty of Technology, University of Portsmouth, Anglesea Building, Anglesea Road, Portsmouth, PO1 3DJ UK.
Sarah DavisSchool of Mechanical & Design Engineering Faculty of Technology, University of Portsmouth, Anglesea Building, Anglesea Road, Portsmouth, PO1 3DJ UK.
Benjamin MorrisonSchool of Mechanical & Design Engineering Faculty of Technology, University of Portsmouth, Anglesea Building, Anglesea Road, Portsmouth, PO1 3DJ UK.
Suleyman KarabalDepartment of Mechanical Engineering, Abdullah Gül University, 38080 Kayseri, Turkey.
Kemal BalandizAlten UK Innovation Laboratory, Alten Limited, 8 Pinnacle Way, Pride Park, Derby, DE24 8ZS UK.
Nigel SmithBioCera Medical Limited, 3B Homefield Road, Haverhill, Suffolk CB9 8QP UK.
Sergey UsovBioCera Medical Limited, 3B Homefield Road, Haverhill, Suffolk CB9 8QP UK.
Pavel ShashkovBioCera Medical Limited, 3B Homefield Road, Haverhill, Suffolk CB9 8QP UK.
Roxane BonithonSchool of Mechanical & Design Engineering Faculty of Technology, University of Portsmouth, Anglesea Building, Anglesea Road, Portsmouth, PO1 3DJ UK.
Gordon BlunnFaculty of Science and Health, School of Medicine, Pharmacy and Biomedical Sciences, University of Portsmouth, St Michael's Building, White Swan Road, Portsmouth, PO1 2DT UK.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Biodegradable magnesium (Mg) alloys are promising for various biomedical applications but their susceptibility to corrosion poses significant challenges. This study systematically examines the microstructural integrity and failure mechanisms of electrochemically deposited phosphate- and fluorine-rich coatings on AZ31 Mg alloy subjected to three-point bending (3 PB) in both non-corrosive and physiological (HBSS) environments. High-resolution digital image correlation (HR-DIC) combined with scanning electron microscopy (SEM) enables in situ visualization and quantitative analysis of crack initiation, evolution, and propagation within the coatings. Our findings reveal that thinner (5 µm) coatings are prone to forming dense networks of fine cracks, while thicker (15 µm) coatings display fewer but wider cracks, with both morphologies strongly governed by localized shear strain. Importantly, cross-sectional analyses after load-holding demonstrate that, while surface cracks initially remain confined within the coating, cracks generated under higher mechanical loading can propagate through the entire coating thickness. These through-thickness cracks create direct pathways for corrosive fluids to access the underlying alloy, serving as initiation sites for stress corrosion cracking within the substrate. Furthermore, our results indicate that fluoride in the coating mitigates rapid corrosion. Overall, the study reveals that coating failure and the formation of through-thickness cracks play a critical role in facilitating localized corrosion and crack initiation within the alloy under combined mechanical and corrosive environments. Graphical Abstract: Supplementary Information: The online version contains supplementary material available at 10.1007/s10853-025-11243-4.

Identifiers

PMID40893464
PMCPMC12397167

What Socratic holds

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LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.