Evidence map›Paper›PMID 41145741›Full record

ArticleMikrochimica acta2025

Multi-material integrated 3D-printed electrochemical detection platform for rapid on-site screening of nimesulide in industrial sewage.

Mateusz Cieślik, Magdalena Rucka, Gilvana P Siqueira, Adrian Koterwa, Michał Rycewicz, Rodrigo A A Muñoz, Robert Bogdanowicz, Jacek Ryl

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Mikrochimica acta, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Mateusz CieślikDivision of Electrochemistry and Surface Physical Chemistry, Faculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk, 80-233, Poland. mateusz.cieslik@ug.edu.pl.
Magdalena RuckaDepartment of Mechanics of Materials and Structures, Faculty of Civil and Environmental Engineering, Narutowicza 11/12, Gdańsk, 80-233, Poland.
Gilvana P SiqueiraDivision of Electrochemistry and Surface Physical Chemistry, Faculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk, 80-233, Poland.
Adrian KoterwaDepartment of Analytical Chemistry, University of Gdańsk, Wita Stwosza 63, Gdańsk, 80-308, Poland.
Michał RycewiczDepartment of Metrology and Optoelectronics, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk, 80-233, Poland.
Rodrigo A A MuñozInstitute of Chemistry, Federal University of Uberlândia, Uberlândia, MG, 38408-100, Brazil. munoz@ufu.br.
Robert BogdanowiczDepartment of Metrology and Optoelectronics, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk, 80-233, Poland.
Jacek RylDivision of Electrochemistry and Surface Physical Chemistry, Faculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk, 80-233, Poland. jacek.ryl@pg.edu.pl.

Funding

Fahrenheit Universities Fahrenheit scholarshipNarodowe Centrum Badań i Rozwoju HYDROSTRATEG1/0006/2022Narodowe Centrum Nauki 2020/38/E/ST8/00409Politechnika Gdańska 2/1/2024/IDUB/I.2b/EsPolitechnika Gdańska 24/1/2022/IDUB/V.5d/VHRPolitechnika Gdańska 3/1/2025/IDUB/IV.2a/Eu
6 · The paper itself

Abstract

The fabrication, mechano-electric, and electrochemical characterisation of a sustainable, multi-material, integrated 3D-printed electrochemical platform (3DPEC) for the rapid on-site screening of nimesulide in both static and flow conditions is demonstrated. The portable two-electrode cell comprises carbon black (CB)-filled polylactic acid (PLA) electrodes sealed within insulating poly(lactic acid) walls, constituting an integrated multi-material system. Joint tensile and electrical tests, as well as tomography analyses, enabled the optimisation of 3DPEC dimensions and printing parameters. A practical and straightforward route for 3DPEC post-processing activation was proposed to enhance the electrochemically active surface area (ESA). Finally, we present the (sensitive determination of nimesulide, an anti-inflammatory drug, in industrial sewage after a 1:10 (v/v) dilution in phosphate buffer solution (PBS). The detection platform demonstrated high competitive performance in electroanalysis, with excellent reproducibility (RSD = 6.8% by CV, 3.4% by DPV), a recovery of 90 ± 5%, a detection limit of 0.19 μM, and selectivity against most studied interferents. The presented approach serves as a proof-of-concept for a customisable, multi-material integrated 3D-printed electrochemical detection platform that prioritises reproducibility, low cost, and applicability in complex environmental matrices, highlighting its practical potential for sustainable wastewater monitoring.

Indexed as

Electrochemical TechniquesPrinting, Three-DimensionalSewageSulfonamidesWater Pollutants, ChemicalElectrodesLimit of DetectionPolyestersReproducibility of ResultsnimesulidePolyesterspoly(lactide)SewageSulfonamidesWater Pollutants, Chemical3D-printed electrochemical cellDifferential pulse voltammetryIndustrial sewageMechano-electric testingNimesulide detectionSustainable sensor

Identifiers

PMID41145741
PMCPMC12559132

What Socratic holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.