ArticleOrganic letters2025
Photoinduced Deoxygenative Boration of Unactivated Alcohols Involving In-Situ-Formed Alkyl Iodides.
Article in Organic letters, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
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Authors and funding
3 authors.
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Abstract
A method for the direct two-step/one-pot conversion of unactivated 1°, 2°, and 3° alcohols into the corresponding alkylboronate esters is reported. The hydroxy group is activated in situ by reaction with the Hendrickson "POP" reagent. The rapidly formed alkoxyphosphonium salt is then reacted with bis(catecholato)diboron under visible-light irradiation in the presence of stoichiometric amounts of lithium iodide. This one-pot protocol streamlines the two-step procedure, and it is operationally simple and scalable. The functional-group tolerance is broad.
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Registered trials
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