Evidence map›Paper›PMID 41228596›Full record

ArticlePolymers2025

Development and Characterization of Scented PLA-Based Biocomposites Reinforced with Spent Coffee Grounds and Lignin for FDM 3D Printing.

Zeineb Siala, Ahmed Koubaa, Sofiane Guessasma, Nicolas Stephant, Ahmed Elloumi, Martin Beauregard

Abstract read
In one paragraph

Article in Polymers, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Article
  2. Article
  3. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Zeineb SialaForest Research Institute, UQAT-Université du Québec en Abitibi-Témiscamingue, 445, boul. de l'Université, Rouyn-Noranda, QC J9X 5E4, Canada.ORCID 0009-0000-9737-6853
Ahmed KoubaaForest Research Institute, UQAT-Université du Québec en Abitibi-Témiscamingue, 445, boul. de l'Université, Rouyn-Noranda, QC J9X 5E4, Canada.ORCID 0000-0002-7895-1901
Sofiane GuessasmaINRAE, UR 1268 Biopolymères Interactions Assemblages, Équipe Paroi Végétale et Polymères Pariétaux, Site de la Géraudière BP71627, CEDEX, 44316 Nantes, France.ORCID 0000-0002-4412-473X
Nicolas StephantInstitut des Matériaux de Nantes Jean Rouxel (IMN), Centre National de la Recherche Scientifique (CNRS), Nantes Université, 44300 Nantes, France.ORCID 0000-0002-6099-5228
Ahmed ElloumiDesign, ISAMS-Institut Supérieur des Arts et Métiers de Sfax, 34 Av. 5 août, Sfax 3069, Tunisia.ORCID 0000-0003-4863-5243
Martin BeauregardCreation and new media, UQAT-Université du Québec en Abitibi-Témiscamingue, 445, boul. de l'Université, Rouyn-Noranda, QC J9X 5E4, Canada.

Funding

Canada Research Chairs 41578
6 · The paper itself

Abstract

This study investigates the development of biodegradable, scented bio-composite filaments incorporating industrial residues, specifically spent coffee grounds (SCG) and lignin (LI), into a PLA matrix for FDM 3D printing. Two fragrance additives, essential oil (EO) and microencapsulated fragrance powder (FP), were introduced (3%) to enhance sensory properties. The research investigates the effects of filler content (5%, 10%, and 15%) and fragrance additives on the surface chemistry (FTIR), thermal stability (TGA and DSC), mechanical properties (Tensile, flexural and impact), microstructure, and dimensional stability (Water absorption test and thickness swelling). Incorporating industrial residues and additives into PLA reduced the thermal stability, the degradation temperature and the glass transition temperature but increased the residual mass and the crystallinity. The effect of lignin was more pronounced than that of SCG, significantly influencing these thermal properties. Increasing the filler content of spent coffee grounds and lignin also led to a progressive decrease in tensile, flexural, and impact strength due to poor interfacial adhesion and increased void formation. However, lignin-based biocomposites exhibited enhanced stiffness at lower concentrations (≤10%), while biocomposites containing 15% SCG doubled their elongation at break compared to pure PLA. Adding fragrance reduced the mechanical strength but improved ductility due to plasticizer-like interactions. Microstructural analysis revealed heterogeneity in the biocomposites' fracture surface characterized by the presence of pores, filler agglomeration, and delamination, indicating uneven filler dispersion and limited interfacial adhesion, particularly at high filler concentrations. The water absorption and dimensional stability of 3D-printed biocomposites increased progressively with the addition of residues. The presence of essential oil slightly improved water resistance by forming hydrogen bonds that limited moisture absorption. This article adds significant value by extending the potential applications of biocomposites beyond conventional engineering uses, making them particularly suitable for the fashion and design sectors, where multi-sensory and sustainable materials are increasingly sought after.

Indexed as

additive manufacturingbiodegradablefragrance additivesfused deposition modelingligninscented biocompositesspent coffee grounds

Identifiers

PMID41228596
PMCPMC12608912

What Socratic holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the Socratic graph.