ArticleMaterials (Basel, Switzerland)2026
Fine Characterization of Co/Fe-Based Materials: Insights into the Influence of Cation Ratios Between 2/2 and 10/2 on Obtaining Layered Double Hydroxides.
Article in Materials (Basel, Switzerland), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Co/Fe layered double hydroxides (LDHs) are among the most promising materials for advanced industrial and energy applications. Controlling the synthesis conditions of LDH materials is thus crucial to precisely tailoring cation composition and distribution, thereby regulating surface charge, ion sorption, and electron transfer required for optimal chemical and electrochemical performance. Therefore, characterizing Co/Fe precipitates (chemical composition, purity, morphology, and crystallinity) is also required to further exploit their controlled properties. Thus, solids with Co/Fe cation ratios between 2/2 and 10/2 were synthesized under an air atmosphere, at pH 8 or 11.5. For the first time, multiscale physicochemical techniques (FTIR, TEM-EELS, SEM, AAS, TGA, CHN elemental analysis, and XRD complemented by Rietveld refinement) were used to provide a fully documented characterization of the structure, texture, purity, chemical composition, and thermal properties of Co/Fe LDH-based materials. The combined interpretation of data from these complementary techniques enabled the precise identification and chemical characterization of the mineralogical phases formed. Both acid-base and redox reactions govern the overall Co
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