ArticleChemSusChem2026
Closing the Carbon Loop: Continuous-Flow Synthesis of N-Aroyl Sulfoximines via Electrochemical CO
Article in ChemSusChem, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Sulfoximines have emerged as versatile scaffolds in modern synthesis, medicinal chemistry, and catalysis due to their tunable electronic and steric properties. In particular, N-aroyl sulfoximines are valuable intermediates in amide coupling, CH functionalization, and heterocycle formation. However, conventional synthetic approaches often rely on stoichiometric activating reagents and harsh conditions, generating waste and limiting substrate scope. Herein, we report a sustainable continuous-flow platform for the Pd-catalyzed carbonylative N-aroylation of sulfoximines employing carbon monoxide (CO) as a C1 source under mild conditions. The system integrates a solid oxide electrolysis cell (SOEC) to generate dry CO from CO
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